

Type of Document Dissertation Author van Gelder, Maarten F. Author's Email Address mvgelder@vt.edu URN etd-12698-1093 Title A Thermistor Based Method for Measurement of Thermal conductivity and Thermal Diffusivity of Moist Food Materials at High Temperatures Degree PhD Department Biological Systems Engineering Advisory Committee
Advisor Name Title Diehl, Kenneth C. Committee Chair Agblevor, Foster Aryi Committee Member Haugh, C. Gene Committee Member Marcy, Joseph E. Committee Member Wilson, James H. Committee Member Keywords
- high temperature
- food material
- thermal diffusivity
Date of Defense 1997-12-18 Availability unrestricted Abstract
A THERMISTOR BASED METHOD FOR MEASUREMENT OF THERMAL
CONDUCTIVITY AND THERMAL DIFFUSIVITY OF MOIST FOOD MATERIALS
AT HIGH TEMPERATURES
by
Maarten F. van Gelder
Kenneth C. Diehl, Jr., Chairman
Biological Systems Engineering
(ABSTRACT)
The purpose of this research was to assess the suitability of
the thermistor based method for measuring thermal conductivity
and diffusivity of moist food materials at high temperatures.
Research focused on aspects of calibration, thermal contact in
solid food materials, natural convection in liquid media and
the performance in moist food materials at high temperatures.
Thermistor probes were constructed in house and calibrated in
three materials of known thermal conductivity and diffusivity,
water, glycerol, and a heat transfer fluid, HTF 500. With few
exceptions, the calibrated probe estimated thermal properties
with an error of less than 5%, over the range of thermal
properties spanned by the those of the calibration media. An
alternate calibration using two media was also investigated. It
was found to give better accuracy over a more limited range.
Thermal contact in potato and lean beef was investigated
through a comparative study that used a miniature line heat
source probe as a reference method. The food materials were
measured at 25, 50 and 100 °C. Good agreement was found between
the measurements with the line heat source probe and the bead
thermistor probe, indicating adequate thermal contact at the
thermistor probe.
The effect of fluid viscosity and the magnitude of the
temperature step on the occurrence of natural convection was
studied for aqueous solutions of a thickening agent. During a
sample time of 30 seconds, convection was absent in solutions
with a viscosity of 25 cp or greater, when measured with a
temperature step of 1.5 and 2.5 °C, and in solutions with a
viscosity of 50 cp or greater, when measured with a temperature
step of 5.0 °C. A Rayleigh number was defined to study the
notion of a critical Rayleigh number at the onset of
convection. This study found that when the Rayleigh number was
below 43, convection could not be demonstrated. For a Rayleigh
number of 84 and higher, convection was observed.
The performance at high temperatures in food materials was
studied through tests in tomato concentrate and in a liquid
food supplement. Tomato puree and tomato paste were sampled at
100, 130 and 150 °C. The thermal conductivity of tomato puree
at 100, 130 and 150 °C was measured as 0.638, 0.645 and 0.647
W/m°C respectively. The thermal diffusivity was 1.63, 1.64 and
1.62 10 -7 m 2 /s respectively. For tomato paste at 100, 130 and
150 °C, a thermal conductivity was obtained of 0.590, 0.597 and
0.534 W/m°C respectively. The thermal diffusivity was 1.63,
1.84 and 2.36 10 -7 m 2 /s respectively. With some notable
exceptions the results of this study agreed well with Choi and
Okos (1983). A liquid food supplement was also studied at 95
and 150 °C. The thermal conductivity of the food supplement
decreased with increasing solids content from 0.62 W/m°C at a
solids level of 15% to 0.41 W/m°C at a solids level of 50%.
The results of this study indicate that the thermistor based
method was suitable for measuring thermal conductivity and
diffusivity of moist food materials at high temperatures.
However, the type of thermistor used in the research, a glass
encapsulated thermistor, was too fragile for routine work. In
particular the high temperature use of the glass thermistor was
impacted by its susceptibility to fracture.
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